Characterization of dyestuffs and metals from selected 16-17th-century ottoman silk brocades by RP-HPLC-DAD and FESEM-EDX


Karadag R., Torgan E., TAŞKÖPRÜ T., Yildiz Y.

Journal of Liquid Chromatography and Related Technologies, vol.38, no.5, pp.591-599, 2015 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 38 Issue: 5
  • Publication Date: 2015
  • Doi Number: 10.1080/10826076.2014.922476
  • Journal Name: Journal of Liquid Chromatography and Related Technologies
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.591-599
  • Keywords: dyestuff, Ottoman silk brocade, metal thread, FESEM-EDX, cultural heritage, HPLC-DAD, PERFORMANCE LIQUID-CHROMATOGRAPHY, DACTYLOPIUS-COCCUS COSTA, DIODE-ARRAY DETECTION, RESEDA-LUTEOLA L., RED NATURAL DYES, TEXTILES, IDENTIFICATION, PIGMENTS, THREADS, WELD
  • Anadolu University Affiliated: No

Abstract

© 2015 Copyright Taylor & Francis Group, LLC.In this study, the analysis of dyestuff and metal thread samples present in the 16-17th-century Ottoman silk textile samples were performed by HPLC-DAD (high-performance liquid chromatography coupled with diode array detection) and FESEM-EDX (field emission scanning electron microscopy with energy dispersion spectroscopy). HPLC-DAD was used for the identification of dyestuffs in different plants and insects such as weld, dyer's oak, walloon oak, woad, indigo, madder, young fustic, and cochineal. Silk yarns with yellow, blue, orange, brown, red, and green colors were selected for the analysis. One of the most useful procedures for fast and simple determination of specific metals of interest is FESEM-EDX. This is a simple method that provides information on chemical composition of sample surfaces and chemical analysis of metal threads.