Optimization of alpha-sialon microstructure by heat treatment

Kurama S.

5th China International Conference on High-Performance Ceramics (CICC-5), Changsha, Çin, 10 - 13 Mayıs 2007, cilt.368-372, ss.891-893 identifier

  • Yayın Türü: Bildiri / Tam Metin Bildiri
  • Cilt numarası: 368-372
  • Doi Numarası: 10.4028/www.scientific.net/kem.368-372.891
  • Basıldığı Şehir: Changsha
  • Basıldığı Ülke: Çin
  • Sayfa Sayıları: ss.891-893
  • Anahtar Kelimeler: SiAlON, heat treatment, image analyze, LSW theory, PROCESSING CONDITIONS, CERAMICS, GRAINS, ADDITIVES
  • Anadolu Üniversitesi Adresli: Hayır

Özet

Nd-doped alpha-SiAlON starting composition (Nd(0.33)Si(9.38)Al(2.62)O(1.62)N(14.38)) was prepared by gas pressure sintering at 1825 degrees C for 3 hrs. In order to explore the effect of post heat treatment on the developments of elongated (alpha-SiAlON grains, sample was heat treated at 1800 degrees C for 4-12 hrs. It was found that post heat treatments promoted formation of the elongated alpha-SiAlON grains. The controlling mechanism of grain growth was determined via plotting on a graph the growth in width/length versus time graphics using Image Analysis method. Different growth rates were found between the length and width direction of the alpha-SiAlON crystals, resulting in anisotropic grain growth in the microstructural development.